已公佈之微波化學標準方法總覽
一. NIEA(中華民國環保署環境檢驗所)之環境檢測標準方法
NIEA C303.01T(1994)
魚介類酸性消化總則－微波消化／元素分析法(Acid Digestion of Fish and Shellfish
Using Closed Vessel Microwave Digestion for Element Determination.)
NIEA W312.50C (2000)
水中金屬元素之萃取－微波輔助酸消化法(Microwave Assisted Acid Leach of Aqueous
Samples and Extracts.)
NIEA A302.70C(2001)
排放管道中重金屬檢測方法 (Determination of Metals Emissions from Stationary Sources.)
NIEA R355.00C (2002)
沈積物、污泥及油脂中金屬元素總量檢測－微波消化原子光譜法（Microwave Assisted
Acid Digestion of Sediments, Sludges, and Oils.）
NIEA R317.10C (2002)
事業廢棄物萃出液中重金屬檢測方法－微波輔助酸消化法（Characterization of Waste-
Microwave Assisted Digestion for Subsequent Determination of Elements in Waste Extracts.）
二. NLDF(中華民國衛生署藥物食品檢驗局)之食品分析標準方法
NLDF 0939300138 (2004)
食品中重金屬檢驗方法-汞之檢驗(二) ：聚焦式微波消化及原子螢光光譜法 (Method
of Test for Heavy Metals in Foods- Test of Mercury (2) : Foused Microwave Digestion and
Atomic Fluroescence Spectrometry)
U.S. EPA Methods (www.epa.gov)
三.USEPA(美國環境保護署)之環境分析標準方法
USEPA NPDES-1992
Guidelines Establishing Test Procedures for the Analysis of Pollutants; Microwave Digestion
– Closed Vessel Microwave Digestion of Wastewater Samples for Metals Determination.
(廢水樣品中金屬元素測定－密閉式微波消化方法)
USEPA 29 -1996
Determination of Metals Emissions from Stationary Sources by Emission Measurement Center.
(排放管道中金屬含量檢測方法－加熱板與密閉式微波消化方法)
USEPA 3050B-1996
Acid Digestion of Sediments, Sludges, and Soils. （土壤、污泥、沈積物中金屬含量測定
－開放式微波酸消化法）
USEPA 3052 -1996
Microwave Assisted Acid Digestion of Siliceous and Organically Based Matrices
(含矽基質與有機物基質的環境樣品－微波輔助酸性消化法)
USEPA 3015A -1998
Microwave Assisted Acid Leach of Aqueous Samples and Extracts.
(水樣及水溶出液中金屬含量測定－微波輔助酸性溶出法)
USEPA 3051A-1998
Microwave Assisted Acid Dissolution of Sediments, Sludges, Soilds, Oils.
（土壤、污泥、沈積物中金屬含量測定－微波輔助酸性溶出法）
USEPA IO-3.1-1999
Selection, Preparation and Extraction of Filter Material－Microwave Extraction Procedure.
(大氣中金屬元素測定中濾紙選擇,製備與微波萃取法)
USEPA 3546 -2000
Standard Procedure for Closed Vessel Microwave Solvent Extracting Water Insoluble or
Slightly Water Soluble Organic Compounds From Soils, Clays, Sediments, Sludges and
Solid Wastes – Microwave Extraction.（土壤、沈積物和固態廢棄物中有機物測定－
微波萃取法）
USEPA 3031
Acid Digestion of Oils for Metals Analysis by Atomic Absorption or ICP Spectrometry.
(油中金屬含量測定之原子吸光或ICP分光儀微波消化法)
USEPA 3200
Mercury Species Fractionation and Quantification by Microwave Assisted Extraction,
Selective Solvent Extraction and/or Solid Phase Extraction. (汞物種分餾與定量方法－
微波輔助萃取法、選擇溶劑萃取法或/與固相萃取法)
USEPA 6800
Elemental and Speciated Isotope Dilution Mass Spectrometry.
(元素與物種同位素稀釋質譜分析法)
四. APHA(美國公共衛生學會)之水與廢水標準檢測方法
APHA 3030K(1992)
The Preliminary Treatment for Metals Determination of Water and Wastewater
– Microwave Assisted Digestion.
(水與廢水中金屬含量測定－微波輔助消化法)
ASTM Methods (www.astm.com)
五.ASTM(美國標準測試與材料協會)之標準分析方法
ASTM E1358-90
Standard Test Method for Determination of Moisture Content of Particulate Woods
Fuels Using a Microwave Oven. (細顆粒狀木材燃料中水份含量－微波烘箱測定法)
ASTM D4309-91
Standard Practice for Sample Preparation using Closed Vessel Microwave Heating
Technique for the Determination of Total Recoverable Metals in Water. (水中金屬含量
測定－微波酸性消化法)
ASTM D5258-92
Standard Practice for Acid Extraction of Elements from Sediments using Closed Vessel
Microwave Heating. (土壤與沈積物中元素之萃取－密閉式微波酸性消化法)
ASTM D4643-93
Standard Test Method for Determination of Water ( Moisture) Content of Soil by the
Microwave Oven Method. (土壤中水份含量－微波烘乾測定法)
ASTM D1506-94b
Standard Test Methods for Carbon Black - Ash Content. (碳煙中灰份含量－微波
灰化測定法)
ASTM D5513-94
Standard Practice for Microwave Digestion of Industrial Furnace Feeds Streams for
Trace Element Analysis. (工業熔爐燃燒進料中微量元素分析－微波消化法)
ASTM D5630-94b
Standard Test Method for Ash Content in Thermoplastics: Procedure B: Rapid –
Ash Muffle Furnace Technique. (熱塑性塑膠中灰份含量－快速微波高溫灰化測定法)
ASTM E1645-94
Standard Practice for the Preparation of Dried Paint Samples for Subsequent Lead
Analysis by Atomic Spectrometry. – Microwave Extraction. (已乾油漆中鉛含量測定
－微波酸性萃取原子光譜法)
ASTM D5765-95
Standard Practice for Solvent Extraction of Total Petroleum Hydrocarbons from
Soils And Sediments Using Closed Vessel Microwave Heating. (土壤與沈積物總石
油烴含量測定–密閉式微波溶劑萃取法)
ASTM D6010-96
Standard Practice for Closed Vessel Microwave Solvent Extraction of Organic
Compounds from Solid Matrices. (固態基質中有機化合物含量測定－密閉式微波
溶劑萃取法)
ASTM D6785
Standard Test Method for Determination of Lead in Workplace Air Using Flame
or Graphite Furnace Atomic Absorption Spectrometry. (作業場所空氣中鉛量－
火焰或石墨爐原子吸光分析法)
ASTM E1741-00
Standard Practice for Preparation of Airborne Particulate Lead Samples Collected
During Abatement and Construction Activities for Subsequent Analysis by Atomic
Spectrometry. (在減輕與建築活動期間採集空氣中粒狀物鉛含量之前處理標準程序
及其原子光譜分析法)
六. CEN(歐洲標準委員會)or BSi(英國標準協會)之標準測定方法
EN 13656:1999
Characterization of Waste – Microwave Assisted Digestion with Hydrofluoric (HF),
Nitric (HNO3) and Hydrochloric (HCl) Acid Mixture for Subsequent Determination
of Elements in Waste. (廢棄物中元素含量測定－微波輔助鹽酸/硝酸與氟酸全消化法)
EN 13657:1999
Characterization of Waste – Digestion for Subsequent Determination of Aqua Regia
Soluble Portion of Elements in Waste. (廢棄物中元素含量測定－密閉或開放式微波
輔助王水溶出消化法)
EN 13346:2000
Characterization of Sludges – Determination of Trace Elements and Phosphorus –
Aqua Regia Extraction Methods. (污泥中微量元素與磷含量測定－密閉或開放式微波
輔助王水萃取法)
七. ISO(國際標準組織)之標準測定方法
ISO 15587:2002
Water Quality – Digestion for the Determination of Selected Elements in Water
– Part 1: Aqua Regia Digestion, Part 2: Nitric Acid Digestion.
(水中金屬元素之萃取消化法－微波輔助王水或硝酸消化法)
八. NIOSH(美國國家職業安全衛生研究所)之分析參考方法
NIOSH 7300 (1994)
Elements in Air by ICP. – Appendix: Microwave Digestion for Lead in Paint Chips and
Other Matrices. (作業環境空氣中元素含量測定－微波消化ICP光譜法)
NIOSH 7082 (1994)
Lead in Air by Flame AAS. – Appendix : Microwave Digestion for Lead in Paint Chips
and Other Matrices. (作業環境空氣中鉛含量測定－微波消化火焰原子光譜法)
NIOSH 7105 (1994)
Lead in Air by GFAAS.– Appendix: Microwave Digestion for Lead in Paint Chips and
Other Matrices. (作業環境空氣中鉛含量測定－微波消化火焰原子/石墨爐光譜法)
九. UOP(環球石油產品科技公司)石油化學之標準測定方法
UOP 291- 89
Total Chloride in Alumina and Silica -Alumina Catalyst by Potentiometric Titration
– Appendix: Microwave Digestion of Catalyst. (電位滴定氧化鋁或矽-氧化鋁觸媒中
總氯化物含量－微波消化法)
AOAC Methods (www.aoac.org)
十. AOAC International(國際公定分析化學家協會)食品分析公定標準方法
AOAC 977.11 (1977)
Moisture in Cheese. – Method Ⅳ: Microwave Oven Method.
(乳酪之水份含量測定法－微波烘乾法)
AOAC 985.14 (1985)
Moisture in Meat and Poultry Products. – Rapid Microwave Drying Method.
(畜禽肉製品之水份含量測定法－快速微波乾燥法)
AOAC 985.15 (1985)
Crude Fat in Meat and Poultry Products. – Rapid Microwave Solvent Extraction Method.
(畜禽肉製品之粗脂肪含量測定法－微波與溶劑萃取)
AOAC 985.26 (1985)
Total Solids in Processed Tomato Products. – Microwave Oven Drying Method.
(蕃茄製品之總固形物含量測定法－微波烘箱乾燥法)
AOAC PVM 1:2003
The Rapid Determination of Fat and Moisture in Meats by Microwave and NMR
Analysis. (肉品中脂肪和水份含量快速測定法－微波與核磁共振法)
AOAC PVM 1:2004
The Rapid Determination of Fat and Moisture in Dairy Products by Microwave and NMR
Analysis. (乳品中脂肪和水份含量快速測定法－微波與核磁共振法)
AOAC 2006.03
Determination of Arsenic, Cadmium, Cobalt, Chromium, Lead, Molydenum, Nickel, and
Selenium in Fertilizer by Microwave Digestion and Inductively Coupled Plasma-Optical
Emission Spectrometry Detection.( 測定肥料中砷、鎘、鈷、鉻、鉛、鉬、鎳、硒含量:
微波消化與ICP光譜分析法)
U.S. Pharmacopeia Methods
(www.usp.org)
十一.美國藥典方法(U.S. Pharmacopeia Methods)
USP 281
Residue on Ignition(藥品之熾灼殘量標準分析方法)
USP 733
Loss on Ignition(藥品之熾灼損失量標準分析方法)
Semiconductor Equipment and Materials
International Methods (www.semi.org)
十二. 國際半導體設備與物料標準方法
SEMI F48-0600
Test Method for Determining Trace Metals in Polymer Materials
(聚合物中微量金屬含量之測定法)
十三. 加拿大健康局香菸菸絲微波消化方法
Health Canada_Official Method/ no. T-306
Determination of Ni,Pb,Cd,Cr,As,Se,Hg in Whole Tobacco(全菸草中 鎳, 鉛,鎘,鉻,砷,硒和汞的檢測)
十四.IEC(國際電子技術標準委員會)之標準測定方法(U.S. Pharmacopeia Methods)
IEC 62321_11
高分子材金屬材及電子電機零件中汞之檢測方法－密閉式微波消化法
IEC 62321_12
電氣設備的高分子元件之Pb,Cd檢測方法－密閉式微波消化法
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